Laboratoire Ingénierie des Fluides Systèmes Énergétiques

The masks have always been mentioned as an effective tool against environmental threats. They are considered as protective equipment to preserve the respiratory system against the non-desirable air droplets and aerosols such as the viral or pollution particles. The aerosols can be pollution existence in the air, or the infectious airborne viruses initiated from the sneezing, coughing of the infected people. The filtration efficiency of the different masks against these aerosols are not the same, as the particles have different sizes, shapes, and properties. Therefore, the challenge is to fabricate the filtration masks with higher efficiency to decrease the penetration percentage at the nastiest conditions. To achieve this concept, knowledge about the mechanisms of the penetration of the aerosols through the masks at different effective environmental conditions is necessary. In this paper, the literature about the different kinds of face masks and respiratory masks, common cases of their application, and the advantages and disadvantages of them in this regard have been reviewed. Moreover, the related mechanisms of the penetration of the aerosols through the masks are discussed. The environmental conditions affecting the penetration as well as the quality of the fabrication are studied. Finally, special attention was given to the numerical simulation related to the different existing mechanisms.

Three-dimensional (3D) bioprinting, an additive manufacturing based technique of biomaterials fabrication, is an innovative and auspicious strategy in medical and pharmaceutical fields. The ability of producing regenerative tissues and organs has made this technology a pioneer to the creation of artificial multi-cellular tissues/organs. A broad variety of biomaterials is currently being utilized in 3D bioprinting as well as multiple techniques employed by researchers. In this review, we demonstrate the most common and novel biomaterials in 3D bioprinting technology further with introducing the related techniques that are commonly taking into account by researchers. In addition, an attempt has been accomplished to hand over the most relevant application of 3D bioprinting techniques such as tissue regeneration, cancer investigations, etc. by presenting the most important works. The main aim of this review paper is to emphasis on strengths and limitations of existence biomaterials and 3D bioprinting techniques in order to carry out a comparison through them.

Abstract Fused filament fabrication is considered one of the most used processes in additive manufacturing rapid prototypes out of polymeric material. Poor strength of the deposited layers is still one of the main critical problems in this process, which affects the mechanical properties of the final parts. To improve the mechanical strength, investigation into various process parameters must be considered. In this article, the influence of different process parameters has been experimentally investigated by means of physicochemical and mechanical characterizations. Special attention was given to the thermal aspect. In that respect, the in situ measurement of temperature profile during deposition indicated that several parameters affect the cooling rate of material and consequently have an influence on the final parts. It was found that the influence of increasing the extruder temperature is more significant in comparison with other process parameters.

Polymer membranes are central to the proper operation of several processes used in a wide range of applications. The production of these membranes relies on processes such as phase inversion, stretching, track etching, sintering, or electrospinning. A novel and competitive strategy in membrane production is the use of additive manufacturing that enables the easier manufacture of tailored membranes. To achieve the future development of better membranes, it is necessary to compare this novel production process to that of more conventional techniques, and clarify the advantages and disadvantages. This review article compares a conventional method of manufacturing polymer membranes to additive manufacturing. A review of 3D printed membranes is also done to give researchers a reference guide. Membranes from these two approaches were compared in terms of cost, materials, structures, properties, performance. and environmental impact. Results show that very few membrane materials are used as 3D-printed membranes. Such membranes showed acceptable performance, better structures, and less environmental impact compared with those of conventional membranes.

Poly(dodecano-12-lactam) (commercially known as polyamide “PA12”) is one of the most resourceful materials used in the selective laser sintering (SLS) process due to its chemical and physical properties. The present work examined the influence of two SLS parameters, namely, laser power and hatch orientation, on the tensile, structural, thermal, and morphological properties of the fabricated PA12 parts. The main objective was to evaluate the suitable laser power and hatching orientation with respect to obtaining better final properties. PA12 powders and SLS-printed parts were assessed through their particle size distributions, X-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), differential scanning calorimetry (DSC), a scanning electron microscope (SEM), and their tensile properties. The results showed that the significant impact of the laser power while hatching is almost unnoticeable when using a high laser power. A more significant condition of the mechanical properties is the uniformity of the powder bed temperature. Optimum factor levels were achieved at 95% laser power and parallel/perpendicular hatching. Parts produced with the optimized SLS parameters were then subjected to an annealing treatment to induce a relaxation of the residual stress and to enhance the crystallinity. The results showed that annealing the SLS parts at 170 °C for 6 h significantly improved the thermal, structural, and tensile properties of 3D-printed PA12 parts.

Anticorrosive protection efficiency of novel tetrafunctional epoxy prepolymer, namely 2,3,4,5-tetraglycidyloxy pentanal (TGP), for mild steel in 1 M HCl medium was assessed through potentiodynamic polarization (PDP), electrochemical impedance spectroscopy (EIS), scanning electron microscope (SEM), energy dispersive X-ray spectroscopy (EDS), contact angle (CA), adsorption isotherm model, temperature effect and thermodynamic parameters. The synthesized TGP was characterized and confirmed by Fourier transform infrared (FTIR) spectroscopy and nuclear magnetic resonance (NMR). The inhibitory efficiencies found at lower concentration of the prepolymer TGP were85% (PDP) and 87.17% (EIS). PDP measurement illustrated that the TGP behaved as a mixed-type inhibitor in the realized solution. SEM and EDS analysis showeda significant decrease in the corrosion of the MS surface in the presence of the inhibitory prepolymer compared with the blank (1 M HCl). Langmuir adsorption isotherm is the most acceptable modelto describe the TGP epoxy prepolymer on the MS area.

Abstract In this study, polyurethane‐films loaded with diclofenac were used to analyze the drug release kinetics and mechanisms. For this purpose, the experimental procedures were developed under static and dynamic conditions with different initial drug loads of 10, 20, and 30%. In the dynamic condition, to better simulate the biological flow, drug release measurements were investigated at flow rates of 7.5 and 23.5 ml/s. These values indicate the flow rate of the internal carotid artery (ICA) for a normal state of a body and for a person during the exercise, respectively. The experimental data were analyzed and adjusted by Higuchi, Korsmeyer–Peppas, First‐order, zero‐order, and Peppas–Sahlin models in order to understand the mechanisms contributed. Finally, drug release mechanisms were specified by investigating the model correlation coefficients. Experimental results showed that increasing the flow rate and initial drug loads enhance drug liberation. In addition, the rate of release is more influenced by the drug dosage in the static state. The analysis revealed that diffusion, burst, and osmotic pressure are the principal mechanisms contributed. Moreover, Fickian type was the dominant mechanism at all duration of release. However, it was discovered using Peppas–Sahlin model that the contribution of the diffusion mechanism decreases with increasing flow rate and initial dosage. Furthermore, the tests at different drug dosages showed that the number of stages in medication release profile is independent of the flow rate and the medicine percentage. One can conclude that the drug release kinetic in static state is more influenced by drug dosage compared with dynamic state.

In this study, two structurally different scaffolds, a polycaprolactone (PCL)/45S5 Bioglass (BG) composite and PCL/hyaluronic acid (HyA) were fabricated by 3D printing technology and were evaluated for the regeneration of dentin and pulp tissues, respectively. Their physicochemical characterization was performed by field emission scanning electron microscopy (FESEM) equipped with energy dispersive spectroscopy (EDS), Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), atomic force microscopy (AFM), contact angle, and compressive strength tests. The results indicated that the presence of BG in the PCL/BG scaffolds promoted the mechanical properties, surface roughness, and bioactivity. Besides, a surface treatment of the PCL scaffold with HyA considerably increased the hydrophilicity of the scaffolds which led to an enhancement in cell adhesion. Furthermore, the gene expression results showed a significant increase in expression of odontogenic markers, e.g., dentin sialophosphoprotein (DSPP), osteocalcin (OCN), and dentin matrix protein 1 (DMP-1) in the presence of both PCL/BG and PCL/HyA scaffolds. Moreover, to examine the feasibility of the idea for pulp-dentin complex regeneration, a bilayer PCL/BG-PCL/HyA scaffold was successfully fabricated and characterized by FESEM. Based on these results, it can be concluded that PCL/BG and PCL/HyA scaffolds have great potential for promoting hDPSC adhesion and odontogenic differentiation.

Passive flow control techniques, and particularly vortex generators have been used successfully in a broad range of aero- and hydrodynamics applications to alter the characteristics of boundary layer separation. This study aims to review how such techniques can mitigate the extent and impact of cavitation in incompressible flows. This review focuses first on vortex generators to characterize key physical principles. It then considers the complete range of passive flow control technologies, including surface conditioning and roughness, geometry modification, grooves, discharge, injection, obstacles, vortex generators, and bubble generators. The passive flow control techniques reviewed typically delay and suppress boundary layer separation by decreasing the pressure gradient at the separation point. The literature also identifies streamwise vortices that result in the transfer of momentum from the free stream to near-wall low energy flow regions. The area of interest concerns hydraulic machinery, whose performance and life span are particularly susceptible to cavitation. The impact on performance includes a reduction in efficiency and fluctuations in discharge pressure and flow, while cavitation can greatly increase wear of bearings, wearing rings, seals, and impeller surfaces due to excessive vibration and surface erosion. In that context, few studies have also shown the positive effects that passive controls can have on the hydraulic performance of centrifugal pumps, such as total head and efficiency. It is conceivable that a new generation of design in hydraulic systems may be possible if simple design features can be conceived to maximize power transfer and minimize losses and cavitation. There are still, however, significant research gaps in understanding a range of impact factors such as manufacturing processes, lifetime, and durability, and essentially how a static design can be optimized to deliver improved performance over a realistic range of operating conditions.

Abstract Fused filament fabrication (FFF) is an additive manufacturing technique that is used to produce prototypes and a gradually more important processing route to obtain final products. Due to the layer‐by‐layer deposition mechanism involved, bonding between adjacent layers is controlled by the thermal energy of the material being printed, which strongly depends on the temperature development of the filaments during the deposition sequence. This study reports experimental measurements of filament temperature during deposition. These temperature profiles were compared to the predictions made by a previously developed model. The two sets of data showed good agreement, particularly concerning the occurrence of reheating peaks when new filaments are deposited onto previously deposited ones. The developed experimental technique is shown to demonstrate its sensitivity to changing operating conditions, namely platform temperature and deposition velocity. The data generated can be valuable to predict more accurately the bond quality achieved in FFF parts.

In this paper, two different views of sociality, one based upon interferences, and the other based upon complementarity, or interdependence, are confronted. The latter is shown to present a number of theoretical advantages over the former, allowing for an account of different types of social actions— influencing, exchange, cooperation—and of how these emerge from structural social conditions. A formal model of dependence relations is presented, and an algorithm for calculating the dependence networks and situations in a multi‐agent context is briefly shown. A simulator of dependence relations, which edits a set of agents (in terms of their goals, actions, and plans) and applies the algorithm to calculate their dependence relations relative to any given goal, is described, and its applications are discussed. Some elementary simulations are exemplified in order to illustrate the experimental application of the simulator in a two‐agent context. Future expansions of the simulator are finally discussed.

Purpose Fused deposition modeling (FDM) draws particular attention due to its ability to fabricate components directly from a CAD data; however, the mechanical properties of the produced pieces are limited. This paper aims to present the experimental aspect of multi-scale damage analysis and fatigue behavior of polylactic acid (PLA) manufactured by FDM. The main purpose of this paper is to analyze the effect of extruder temperature during the process, loading amplitude, and frequency on fatigue behavior. Design/methodology/approach Three specific case studies were analyzed and compared with spool material for understanding the effect of bonding formation: single printed filament, two printed filaments and three printed filaments. Specific experiments of quasi-static tensile tests coupled with microstructure observations are performed to multi-scale damage analysis. A strong variation of fatigue strength as a function of the loading amplitude, frequency and extruder temperature is also presented. Findings The obtained experimental results show the first observed damage phenomenon corresponds to the inter-layer bonding of the filament interface at the stress value of 40 MPa. For instance, fatigue lifetime clearly depends on the extruder temperature and the loading frequency. Moreover, when the frequency is 80 Hz, the coupling effect of thermal and mechanical fatigue causes self-heating which decreases the fatigue lifetime. Originality/value This paper comprises useful data regarding the mechanical behavior and fatigue lifetime of FDM made PLA specimens. In fact, it evaluates the effect of process parameters (extruder temperature) based on the nature of FDM that is classified as a thermally-driven process.

Fused filament fabrication (FFF), an additive manufacturing technique, unlocks alternative possibilities for the production of complex geometries. In this process, the layer-by-layer deposition mechanism and several heat sources make it a thermally driven process. As heat transfer plays a particular role and determines the temperature history of the merging filaments, the in-process monitoring of the temperature profile guarantees the optimization purposes and thus the improvement of interlayer adhesion. In this review, we document the role of heat transfer in bond formation. In addition, efforts have been carried out to evaluate the correlation of FFF parameters and heat transfer and their effect on part quality. The main objective of this review paper is to provide a comprehensive study on the in-process monitoring of the filament’s temperature profile by presenting and contributing a comparison through the literature.

Abstract Fused filament fabrication process presents drawbacks in mechanical properties observed when printing in the build direction (Z‐direction). Such anisotropic properties will affect the part's performances and have to be minimized during fabrication. This study aims to evaluate the effects of nozzle temperature, printing speed and specimen state (annealed or as‐printed) on porosity percentage and tensile properties for 3D printed polyetherimide (PEI) (ULTEM 1010) parts in Z‐direction. The results demonstrated that print speed is the most influential process parameter that should be adjusted in consideration with the other printing parameters. The specimens' state did not reveal a noticeable influence, as the amorphous nature of PEI is considered less receptive to annealing. The optimization method to achieve the best results yielded values of 360°C and 30 mm s −1 as printing conditions, followed by heat treatment. This was confirmed by porosity measurements, tensile testing, and scanning electron microscopy observations. The best performances of PEI material were 3425.5 MPa, 102 MPa, and 4.30% for Young's modulus, tensile strength, and elongation at break, respectively.

Abstract Fused filament fabrication (FFF), an additive manufacturing technique, is used to produce prototypes and a gradually more important processing route to get final products. Due to the layer‐by‐layer deposition mechanism involved, bonding between adjacent layers is controlled by the thermal energy of the material being printed. Thus, it is strongly in conjunction with the temperature development of the filaments during the deposition sequence. This study gives out an in‐process set‐up enabling to record temperature profile of two adjacent filaments or a sequence of deposition in various locations during FFF process. The main characteristic of the presented procedure is the possibility of obtaining a global temperature profile resulted from an IR‐camera; parallel to those recorded using a K‐type thermocouple. Needless to say that a K‐type thermocouple accurately records the local temperature at the interface of adjacent filaments. Conversely, an IR‐camera signifies the temperature profile on the captured surface. The obtained results showed that there is a remarkable difference between the cooling rate and re‐heating peaks. The primary outcome of this study is the consideration of results accuracy and the possibility of working on optimization of the obtained temperature profile. Altogether it helps optimize inter‐layer strength while assessing the temperature evolution.

Despite the application of the Additive Manufacturing process and the ability of parts’ construction directly from a 3D model, particular attention should be taken into account to improve their mechanical characteristics. In this paper, we present the effect of individual process variables and the strain-rate sensitivity of Onyx (Nylon mixed with chopped carbon fiber) manufactured by Fused Filament Fabrication (FFF), using both experimental and simulation manners. The main objective of this paper is to present the effect of the selected printing parameters (print speed and platform temperature) and the sensitivity of the 3D-printed specimen to the strain rate during tensile behavior. A strong variation of tensile behavior for each set of conditions has been observed during the quasi-static tensile test. The variation of 40 °C in the platform temperature results in a 10% and 11% increase in Young’s modulus and tensile strength, and 8% decrease in the failure strain, respectively. The variation of 20 mm·s−1 in print speed results in a 14% increase in the tensile strength and 11% decrease in the failure strain. The individual effect of process variables is inevitable and affects the mechanical behavior of the 3D-printed composite, as observed from the SEM micrographs (ductile to brittle fracture). The best condition according to their tensile behavior was chosen to investigate the strain rate sensitivity of the printed specimens both experimentally and using Finite Element (FE) simulations. As observed, the strain rate clearly affects the failure mechanism and the predicted behavior using the FE simulation. Increase in the elongation speed from 1 mm·min−1 to 100 mm·min−1, results in a considerable increase in Young’s modulus. SEM micrographs demonstrated that although the mechanical behavior of the material varied by increasing the strain rate, the failure mechanism altered from ductile to brittle failure.

Impellers are referred to as a core component of turbomachinery. The use of impellers in various applications is considered an integral part of the industry. So, increased performance and the optimization of impellers have been the center of attention of a lot of studies. In this regard, studies have been focused on the improvement of the efficiency of rotary machines through aerodynamic optimization, using high-performance materials and suitable manufacturing processes. As such, the use of polymers and polymer composites due to their lower weight when compared to metals has been the focus of studies. On the other hand, methods of the manufacturing process for polymer and polymer composite impellers such as conventional impeller manufacturing, injection molding and additive manufacturing can offer higher economic efficiency than similar metal parts. In this study, polymeric and polymer composites impellers are discussed and conclusions are drawn according to the manufacturing methods. Studies have shown promising results for the replacement of polymers and polymer composites instead of metals with respect to a suitable temperature range. In general, polymers showed a good ability to fabricate the impellers, however in more difficult working conditions considering the need for a substance with higher physical and mechanical properties necessitates the use of composite polymers. However, in some applications, the use of these materials needs further research and development.

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In this study, we present a method for prediction of the drug-release profile based on the physical mechanisms that can intervene in drug release from a drug-carrier. The application presented here incorporates the effects of drug concentration and Reynolds number defining the circulating flow in the testing vein. The experimental data used relate to the release of diclofenac from samples of non-degradable polyurethane subjected to static and continuous flow. This case includes simultaneously three mechanisms: burst-release, diffusion and osmotic pressure, identified beforehand here as being able to contribute to the drug liberation. For this purpose, authors coded the Sequential Quadratic Programming Algorithm to solve the problem of non-linear optimization. The experimental data used to develop the mathematical model obtained from release studies carried out in water solution at 37 °C, for three concentrations of diclofenac and two water flow rates. We discuss the contribution of mechanisms and kinetics by considering two aforementioned parameters and, following that, we obtain the specific-model and compare the calculated results with the experimental results for the reserved cases. The results showed that drug percentage mostly affect the burst release, however flow rate has affected the osmotic release. In addition, release kinetics of all the mechanisms have increased by increasing the values of two considered parameters.

Water Distribution Networks (WDNs) represent a noteworthy field for possible implementation of Small Hydropower (SHP), by replacing Pressure Reduction Valves (PRV) with turbomachines, in particular Pump as Turbines (PaTs), to control and regulate the pressure, while harvesting energy otherwise wasted. Different models were developed to predict the performance and select the positioning of the PaTs for the maximum energy recovery but most of them neglect practical aspect such as: power grid limitations and optimal harvesting strategy. In this framework, we intend to propose a new method to select a PaT, defining its optimal working point, by introducing an energy exploitation coefficient. The proposed methodology is based on the experimental results of a real PaT tested in the high capacity hydraulic laboratory at Polytechnic University of Bari. Firstly, the selected commercial centrifugal pump was tested in both pump and turbine modes. Then, three different approaches, for the Best Efficiency Point (BEP) selection, are described and compared in terms of energy exploitation and capacity factor for a WDN. The first consists of selecting the BEP at the average flow rate, the second one considers the probability distribution of the flow rate and the corresponding available hydraulic energy, whereas the latter is based on the highest energy harvesting. By applying energy production, economic and environmental analyses, the new proposed methodology, based on the third approach, shows a remarkable advantage in terms of exploited energy. Indeed a remarkable 60% energy recovery is achieved with 334 ton CO2/year avoided. Furthermore, the impact of the electrical motor on the maximum power generation (cut-off) is considered. Eventually, useful insights for the future PaT selection and installation are discussed.