Mechanochemical Synthesis of Metal−Organic Frameworks: A Fast and Facile Approach toward Quantitative Yields and High Specific Surface Areas

Klimakow, Maria; Klobes, P.; F. Thünemann, Andreas; Rademann, Klaus; Emmerling, Franziska

doi:10.1021/cm1012119

Public

Mechanochemical Synthesis of Metal−Organic Frameworks: A Fast and Facile Approach toward Quantitative Yields and High Specific Surface Areas

Shared by NobleBlocks on Aug 30, 2010 • 12:00 AM UTC

Authors:

Maria Klimakow

P. Klobes

Andreas F. Thünemann

Abstract

The strategy of utilizing mechanochemical synthesis to obtain metal−organic frameworks (MOFs) with high surface areas is demonstrated for two model systems. The compounds HKUST-1 (Cu3(BTC)2, BTC = 1,3,5-benzenetricarboxylate) and MOF-14 (Cu3(BTB)2, BTB = 4,4′,4′′-benzenetribenzoate) were synthesized...

Subject

Metal-organic framework

Materials science

Small-angle X-ray scattering

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